Sample
Preparation and analyzing.
photo mosaic Samples are first digested
in acid and diluted appropriately. Analysis is
performed using either an Inductively-Coupled Plasma
Atomic Emission Spectrometer or
an Inductively-Coupled Plasma Mass Spectrometer. For
both instruments, the sample is introduced into a plasma of argon
atoms. The temperature of the plasma is approximately
10,000 degrees Celcius! At this temperature the components of the
sample are atomized and promoted to a higher energy
state. The atomic emission spectrometer measures the characteristic color of
light given off by each element as they relax
back to a lower energy level. The mass spectrometer separates and measures
the ionized elements according to the ratio of
mass to charge. With both techniques, the intensity of the measurements for
each sample is compared to a series of
standards and the concentration of each element is
calculated to a high degree of
accuracy.
The Inductively-Coupled
Plasma Atomic Emission Spectrometer is used primarily
for samples known to have relatively high concentrations of the elements of
interest. However, the Inductively-Coupled Plasma
Mass Spectrometer is a more ophisticated instrument used for the detection of
extremely trace levels of elements. Using the
Inductively-Coupled Plasma Mass Spectrometer, we are able to detect
elements at the sub-parts-per-billion level!
TRACE ELEMENT ANALYSIS :
Mass Spectroscopy (ICP MS)
efficienty and accurately determines the level of
toxic exposure in blood, urine and hair samples
with a capability to accurately
measure toxic and trace elements in the part
per billion (ppb) or microgram per liter range. For
certain elements, the detection
is in the part per trillion range.
MINERAL ANALYSIS or MACRO
ELEMENTAL ANALYSIS is performed via ICP
Spectroscopy, a highly accurate measurement of elements that are
present in hair, blood or urine in the part per
million or mg/L range.